Protactinium generator
Here are the results we obtained in class on 6 February 2013 in an experiment to plot the decay curve of protactinium-234 obtained by "milking" this isotope from solution in a protactinium generator.
Method

The Protactinium generator is ideal for demonstrating radioactive decay, as the half life of the Pa-234m isotope is about 70 s, meaning that a decay curve can be plotted in 5-10 mins. Either a datalogger and GM tube sensor or a standard GM tube and counter may be used. [CREDIT: Timstar online catalogue]
Results
Under construction (I seem to have misplaced the results!)
The raw data are shown in the table below, and are also available as a tab delimited text file.
t / s | count / 30-1 s-1 | corrected count / 30-1 s-1 |
---|---|---|
15 | 171 | 166 |
45 | 141 | 136 |
75 | 113 | 108 |
105 | 91 | 86 |
135 | 80 | 75 |
165 | 52 | 47 |
195 | 40 | 35 |
225 | 33 | 28 |
255 | 38 | 33 |
285 | 33 | 28 |
315 | 24 | 19 |
345 | 21 | 16 |
375 | 22 | 17 |
405 | 20 | 15 |
435 | 20 | 15 |
465 | 21 | 16 |
495 | 13 | 8 |
Links
The following links might be of use to enable you to find out more about this experiment:
- Radiochemistry: Decay of protactinium-234m, Peter Keutsch, Universität Regensburg
- Protactinium generator, Nuffield foundation Practical Physics
- Datalogging setup, Youtube video from ScienceScope